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This resin has the unique ability to adsorb strong mineral acids yet exclude metal salts This is not an ion exchange process since only water is used, in a countercurrent fashion, to desorb the acid from the resin 60523 In-tank Electrolytic Permanganate Regeneration Because permanganate is a powerful oxidizing agent only in basic conditions, desmear solutions usually contain 5 to 10 percent caustic soda However, the alkalinity at high temperatures causes the permanganate (MnO4 1) ion to break down to manganate The manganate reacts with water to form manganese dioxide (MnO2), eventually forming a black sludge of MnO2 which settles to the bottom of the desmear tank This requires that the bath be dumped Oxidizing electrolytic regeneration systems are available to inhibit this reaction.

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A typical electrolytic regeneration system employs an in-tank probe composed of a copper rod as the cathode which is connected to a power supply When current is applied, oxygen is generated in the permanganate solution which functions as the regenerate for the manganate The efficiency of the system depends on the rate of manganate buildup, the amount of amperage generated, and the power supply to the in-tank regenerator These probes attach to the top rim of the desmear tank and are always operating (as the permanganate ions will break down even when the bath is not active) In most cases, the use of this equipment has eliminated the need to dump this bath 60524 Proper Rack Design and Maintenance.

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By using plastic-coated racks, only the tips and contactors (which electrically and physically connect and support the panel to the carrying rack), have exposed conductive metal and must be stripped If one of these is removable, then the amount of metal to be chemically or electronically removed from the rack is also reduced This should lengthen the useful life of the stripping bath and further reduce the cost for hauling away or on-site treatment (if nitric acid is used) of the spent rack stripper Use of racks with disposable contactors eliminates the need to strip the racks and could eliminate the use of nitric acid 60525 Dragout Recovery Tanks The dragout tank s primary purpose is to collect most of the solution dragout before the panel enters the rinse tank The dragout (recovery) tank is a rinse tank that operates without a continuous flow of feed water.

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It is positioned between a process bath and its rinse tank The dragout tank can be either an immersion application (for the electroless and innerlayer operations) or a spray type application (on conveyorized equipment or for pattern- or panel-plating operations) After the panels have been removed from the process bath, they are immersed or sprayed in the dragout tank before they are rinsed in another tankThe concentrated rinse water can be collected separately from its following rinse..

Eventually, the concentration of the tank solution will increase to a point such that it provides an opportunity to 1. Recover metals. 2. Recycle a process bath since it is the same chemistry. The disadvantage is that this opportunity may require additional production floor space. A drip pan (also called a drain board) is one of the simplest methods for dragout recovery. The drip pan is located either under the rack while in transit or between tanks, and will capture drips of process solution from racks and panels as these are transferred between tanks. Drip pans not only save chemicals and reduce rinse water requirements, they also improve housekeeping by keeping the floor dry. 60.5.2.6 Monitor Solution Activity. Bath life can be extended by monitoring the bath activity and replenishing stabilizers and reagents. This will reduce dump frequencies and result in a reduction in waste.

Dragout Reduction Dragout reduction is desirable as a waste minimization step because it results in the saving of process chemicals as well as a reduction in sludge generation 60531 Etcher Design Etching machines can be the single largest source of copper waste in the discharge from a PCB facility The amount of copper discharged and the rinse flow rate from that machine are a function of the machine design An older etching machine often contains a single-stage etchant replenishing module positioned between the etching chamber and its continuously flowing single or multiple-stage water rinse chamber Fresh etchant is fed to the replenishing module to wash the panels and that etchant (now containing copper washed off of the freshly etched panels), then flows (in a direction opposite to the direction of the panel movement) into the etching chamber.

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