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ion diffusion potential, allowing the copper to deposit rapidly on an HSA cathode from wastes with both high and low copper concentrations. HSA cathodes promote solution agitation by creating numerous bonding sites for copper. Expanded mesh carbon fibers or catalyzed foam are typical materials of construction in HSA cathodes. Some HSA systems require the purchase of new cathodes, while the cathodes in some systems can be regenerated for a period of time. To regenerate these cathodes they must be stripped of copper metal. Stripping the cathode takes place in a second plating tank. The cathodes from the first tank must be manually removed and placed into the anodic position within the stripping tank. The copper is then recovered as a metal by electroplating the copper onto either a stainless steel or a copper laminate in a copper pyrophosphate electrolyte. The reusable cathodes are then available to be repositioned back to the first cell. HSA systems can reduce the copper levels to low levels in an incoming waste stream, but it is important to note that copper is not recovered unless the stripping step takes place in the second plating tank. 60.6.3.5 Point-of-Source Systems. Dragout tanks can be located between a process bath (for example, a copper-plating bath in the pattern-plating line) and its following rinse tank. Typically, dragout tanks are positioned only adjacent to the process tanks containing the most difficult wastes. These include the etching baths (if not conveyorized), the microetch baths (which produce the most copper), and the copper electroplating (usually sulfate-based) baths. The contents of each dragout bath can be recirculated through its own plating cell for copper recovery, then back to the dragout tank. In this way, the concentration of copper is

maintained at a low level. The plating cell, for this application, could be either a parallel plate or an HSA system. If dedicated electroplating cells are not used to recover copper directly from a dragout bath, the dragout bath can periodically be discharged to a dilute (or concentrated) copper collection tank for recovery through an ion exchange system (or a central electroplating system, respectively).

The graph can also be animated using AnimationOnDisplay and MarkerTooltipType, the latter of which can be used to display information as the mouse is moved over a bar, also shown in Figure 16-2. Other properties such as EmptyText can be used to define a message if there is no graph data, and DynamicResize will automatically stretch the graph within its parent container.

Selective Ion Exchange Ion exchange is a process in which ions, which are held by electrostatic forces to charged functional groups on the surface of the ion exchange resin, are exchanged for ions of similar charge in a solution in which a resin is immersed. Ion exchange is classified as an adsorption process because the exchange occurs on the surface of a solid (a resin bead), and the exchanging ion must undergo a phase transfer from the solution phase to the surface of the solid. A single-pass selective cation exchange column can reduce the copper concentration in the influent stream to less than 1.0 mg/l. If two cation exchange columns are in series, as indicated in Fig. 60.4, the expected copper effluent concentration should be less than 0.5 mg/l. Organics present in the incoming waste can foul the resin and render it unusable; therefore, a carbon filtration step occurs ahead of the ion exchange column.Wastes with significant levels of organic material are not treated with this technology. 60.7.1.1 Theory of Operation. Copper ions are normally present in their divalent (+2) state. The removal mechanism of divalent copper from an aqueous waste by ion exchange resins is: Cu+2 + 2R-H 2H+ + R2-Cu >> (60.5)

where R = a cation exchange resin. Here the copper is attached to the resin beads. Ion exchange equipment suppliers will usually furnish a water meter that totalizes the quantity of waste processed through the column. After the system has been calibrated by the equipment supplier, the water meter will activate an alarm after a specified volume of waste has been processed. An alarm will sound if the system requires manual regeneration. If the system is supplied with automatic regeneration, the water meter will deactivate a column while regeneration takes place. Where multiple columns are included within a system, valves must be adjusted to accommodate regeneration.This will be accomplished by manual or automated (pneumatic-, electric-, or hydraulic-actuated) techniques. 60.7.1.2 Regeneration. To recover the copper, the cation resins are first rinsed with water and then washed with 5 to 15 percent by volume sulfuric acid. This proceeds by the following reaction: R2-Cu + 2H+1 Cu+2 + 2R-H >> (60.6)